Qualitative Analysis of The purpose of this experiment is to demonstrate the separation and identification of metal ions based on the insolubility of certain salts. The solubility rules should be taken into account. If a solution dissolves in water, the result contains both cations and anions. Analyzing different ions to discover their nature is the main goal of this experiment. Separation of the cations by testing the differences in solubility of different metal salts is done. Also, identification of the metal ions is done by the flame test procedure and by the characteristic reaction procedure.
Both of the separation and identification methods will be used. Separation procedure will be done by the methods of decanting or centrifuging. HCl is currosive & toxic. It can cause burns Most of the solutions are poisonous and all should be treated as if they are. 1. Obtain 6ml of the unknown solution.
In a graduated cylinder. 3. Add 5 drops of the unknown solution into each of the test tubes. 1. Add approximately 3 drops of Na2CO3 solution to the solution in test tube one. Thoroughly mix. If the solution turns into a white precipitate then it includes ions from set 2. Record the result.
The Essay on Determine The Macromolecules Present In An Unknown Solution
Every living thing is dependent on large complex molecules, known as macromolecules. The objective of this lab was to correctly identify which macromolecules the unknown solution was comprised of using various substances as experimental controls. There are four major types of biological macromolecules – carbohydrates, lipids, proteins, and nucleic acids – made up of elements such as ...
Waste Disposal- there should be waste bottles under the fume hood. Dispose of solution in a labeled Na2CO3 mixture waste bottle. 2. In test tube two add 5 drops of 1M HCL to the unknown solution. Thoroughly mix. If the solution turns to a white precipitate, it has ions from set 1 . If it turns to a yellowish/red precipitate, it has ions from set 2.
Record the results. Waste Disposal- discard in a labeled HCL mixture waste bottle. 3. In test tube three add approximately 3 drops of 1M NaOH. If the solution turns to a brown precipitate it has ions from set 1, if the solution has a white precipitate it has ions from set 2, if the solution has a blue,green, or red precipitate it has ions from set 3. Record Observations.
Waste Disposal – discard in a NaOH labeled mixture waste bottle. 1. To separate the ions decanting, should be used or a beral pipet. 2. The ions should be separated completely. Waste disposal- place the remaining liquid in the appropriate labled waste container. 1.
If a precipitate forms proceed with the following steps. 2. In each test tube with a precipitate add 4-5 drops of K4[Fe(CN)6]. If the solution turns white it has Ag ion, if the solution turns yellow it has Ba & Ca ions, if the solution turns blue it has Fe ions, if the solution turns red it has Cu or Co ions. Record the result. 3.
In the test tubes without reactions add 4-5 drops of K2CrO4 (keep in fume hood).
If the solution turns red it has the Ag ion, & if the solution turns yellow it has the Pb ion. 5. Next add 4-5 drops of DMG to the solution without reactions. If the solution turns bright red then it has the Ca ion, if the solution turns pink it has the Ni ion. Record the result.
1. Dip the Nichrome wire into 6M HCL shake it around, not too vigorously, and rinse with distilled water. 2. Make a suitable flame with the bunsen burner. Dip the wire in the test tube with no reaction in the unknown solution. 3.
Swipe it through the flame and use a Blue Cobalt glass to view the color. If the color is blue it has the Pb ion, if the color is green it has the Ba ion, if the color is yellowish/red, it has the Ca ion , if the color is bluish green then it has the Cu ion, if the color is red violet it has the Li ion, if the color is purple red it has the K ion. Record the observations. 4. Dip the wire in the 6M of HCL again when cool & rinse with distilled water. Waste Disposal- the remainding solution should be placed in the appropriate containers. The unknown solution is contains .
The Essay on Standardizing A Solution Of Potassium Hydroxide
Abstract: In this lab, a prepared solution of Potassium Hydroxide will be standardized. The solution we will be standardized by performing multiple calculations to ensure the upmost accuracy. The acid used for this titration will be KHP (C4H5KO4). Phenolphthalein we be added to the beaker of the dissolved acid before the titration will be added. The titration will stop when the solution turns pink ...